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Jun Sato, Victor Breedveld
Evaporation Blocker for Cone-Plate Rheometry of Volatile Samples
Appl. Rheol. 15:6 (2005) 390-397
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We report on the design and implementation of an evaporation blocker for cone-plate and plate-plate geometries.
In addition to minimizing sample evaporation by trapping the saturated vapor inside a sample chamber,
an important feature of the evaporation blocker is the suppression of solvent transport through condensation.
Validation tests with DI-water, hydrogels, and colloidal suspensions demonstrate that the new accessory reduces
solvent evaporation significantly more than commercially available environmental control chambers. Experiments
were also performed to show that the evaporation blocker enables a variety of experiments on thermoresponsive
complex fluids that were previously impossible, and provide new insight into the molecular organization
of these materials. The evaporation blocker was specifically designed for an Anton Paar MCR rheometer,
but the fundamental principles are widely applicable.
► Cite this publication as follows:
Sato J, Breedveld V: Evaporation Blocker for Cone-Plate Rheometry of Volatile Samples, Appl. Rheol. 15 (2005) 390.
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